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4-Morpholinecarboxylic acid, 2-[(acetylthio)methyl]-, 1,1-dimethylethyl ester synthesis

2synthesis methods
4-Morpholinecarboxylic acid, 2-[[(methylsulfonyl)oxy]methyl]-, 1,1-dimethylethyl ester

503455-72-9
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10387-40-3 Synthesis
Potassium thioacetate

10387-40-3
343 suppliers
$10.00/1g

4-Morpholinecarboxylic acid, 2-[(acetylthio)methyl]-, 1,1-dimethylethyl ester

933477-81-7
3 suppliers
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Yield:933477-81-7 77%

Reaction Conditions:

in N,N-dimethyl-formamide at 95; for 12 h;

References:

Zhersh, Sergey A.;Blahun, Oleksandr P.;Sadkova, Iryna V.;Tolmachev, Andrey A.;Moroz, Yurii S.;Mykhailiuk, Pavel K. [Chemistry - A European Journal,2018,vol. 24,# 33,p. 8343 - 8349] Location in patent:supporting information