2-(4,5-DIHYDRO-1H-IMIDAZOL-2-YL)-4,5-DIHYDRO-1H-IMDAZOLE synthesis
4synthesis methods
- Product Name:2-(4,5-DIHYDRO-1H-IMIDAZOL-2-YL)-4,5-DIHYDRO-1H-IMDAZOLE
- CAS Number:934-03-2
- Molecular formula:C6H10N4
- Molecular Weight:138.17
Yield:934-03-2 77%
Reaction Conditions:
Stage #1: dithiooxamidewith ethyl bromide in ethanol at 60; for 4 h;Inert atmosphere;Schlenk technique;
Stage #2: ethylenediamine in ethanol at 60 - 80; for 1.33333 h;Inert atmosphere;Schlenk technique;
References:
Léval, Alexander;Agapova, Anastasiya;Steinlechner, Christoph;Alberico, Elisabetta;Junge, Henrik;Beller, Matthias [Green Chemistry,2020,vol. 22,# 3,p. 913 - 920] Location in patent:supporting information
