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Tert-Butyl 7-Methyl-5-Oxo-1,4-Diazepane-1-Carboxylate synthesis

1synthesis methods
24424-99-5 Synthesis
Di-tert-butyl dicarbonate

24424-99-5
820 suppliers
$13.50/25G

90673-37-3 Synthesis
5H-1,4-Diazepin-5-one,hexahydro-7-methyl-(7CI)

90673-37-3
31 suppliers
$117.00/50mg

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Yield:935843-58-6 95%

Reaction Conditions:

with N-ethyl-N,N-diisopropylamine in 1,4-dioxane;water at 20; for 48 h;

References:

Wlodarczyk, Nicolas;Gilleron, Pauline;Millet, Régis;Houssin, Raymond;Hénichart, Jean-Pierre [Tetrahedron Letters,2007,vol. 48,# 14,p. 2583 - 2586]