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N,N-Dimethyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1h-imidazole-1-sulfonamide synthesis

2synthesis methods
-

Yield:942070-58-8 82%

Reaction Conditions:

with (1,5-cyclooctadiene)(methoxy)iridium(I) dimer;4,4'-di-tert-butyl-2,2'-bipyridine in diethyl ether at 20; for 65 h;Inert atmosphere;regioselective reaction;

References:

Kallepalli, Venkata A.;Shi, Feng;Paul, Sulagna;Onyeozili, Edith N.;Maleczka Jr., Robert E.;Smith III, Milton R. [Journal of Organic Chemistry,2009,vol. 74,# 23,p. 9199 - 9201] Location in patent:supporting information; experimental part