![](/CAS/20210111/GIF/946753-98-6.gif)
N~1~-(5-amino-2-methylphenyl)-N~2~,N~2~-dimethylglycinamide(SALTDATA: FREE) synthesis
- Product Name:N~1~-(5-amino-2-methylphenyl)-N~2~,N~2~-dimethylglycinamide(SALTDATA: FREE)
- CAS Number:946753-98-6
- Molecular formula:C11H17N3O
- Molecular Weight:207.27
![Carbamic acid, N-[3-[[2-(dimethylamino)acetyl]amino]-4-methylphenyl]-, 1,1-dimethylethyl ester](/CAS/20210305/GIF/1172621-17-8.gif)
1172621-17-8
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![N~1~-(5-amino-2-methylphenyl)-N~2~,N~2~-dimethylglycinamide(SALTDATA: FREE)](/CAS/20210111/GIF/946753-98-6.gif)
946753-98-6
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$110.00/1g
Yield:946753-98-6 72.4%
Reaction Conditions:
with hydrogenchloride in 1,4-dioxane at 25; for 2 h;
Steps:
24.B
To a solution of tert-butyl 3-(2-(dimethylamino)acetamido)-4-methylphenylcarbamate (0.615 g, 2 mmol) in 1,4-dioxane (2 mL) was added 4N HCl in 1,4-dioxane (2 mL). The solution was stirred at 25°C for 2 hours. Filtration provided the title compound as a white solid (0.30 g, 1.447 mmol, 72.4% yield); 1H NMR (400 MHz, DMSO-d6) δ 10.44 (s, 2H), 10.18 (br. s.,
References:
WO2009/89042,2009,A1 Location in patent:Page/Page column 120-121