ChemicalBook CAS DataBase List Bis{4-[ethyl-(2-hydroxyethyl)carbamoyl]benzyl} Trithiocarbonate

Bis{4-[ethyl-(2-hydroxyethyl)carbamoyl]benzyl} Trithiocarbonate synthesis

3synthesis methods

Product Name:Bis{4-[ethyl-(2-hydroxyethyl)carbamoyl]benzyl} Trithiocarbonate
CAS Number:948877-09-6
Molecular formula:C25H32N2O4S3
Molecular Weight:520.73

876-08-4
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Bis{4-[ethyl-(2-hydroxyethyl)carbamoyl]benzyl} Trithiocarbonate

948877-09-6
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Yield:-

Steps:

Multi-step reaction with 4 steps
1.1: tetrahydrofuran / 4 h / 0 - 20 °C
2.1: dmap; triethylamine / toluene / 2 h / 20 °C
3.1: potassium carbonate / N,N-dimethyl-formamide / 0.25 h / 50 °C
3.2: 24 h / 50 °C
4.1: potassium hydroxide / water / 4 h / 0 - 20 °C

References:

Sudo, Atsushi;Hamaguchi, Takaaki;Aoyagi, Naoto;Endo, Takeshi [Journal of Polymer Science, Part A: Polymer Chemistry,2013,vol. 51,# 2,p. 318 - 326]

BIS{4-[ETHYL-(2-ACETYLOXYETHYL)CARBAMOYL]BENZYL} TRITHIOCARBONATE

948877-08-5
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948877-09-6
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References

Benzamide, 4-(chloromethyl)-N-ethyl-N-(2-hydroxyethyl)-

948877-06-3
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948877-09-6
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References