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D-THREO-PENTONIC ACID, 2-DEOXY-2,2-DIFLUORO-4,5-O-(1-METHYLETHYLIDENE)-, ETHYL ESTER synthesis

1synthesis methods
-

Yield:95058-93-8 20 g ,95058-92-7 65%

Reaction Conditions:

with zinc in tetrahydrofuran;diethyl ether; for 1 h;Heating;

References:

Hertel;Kroin;Misner;Tustin [Journal of Organic Chemistry,1988,vol. 53,# 11,p. 2406 - 2409]