5-(4,4,5,5-TETRAMETHYL-[1,3,2]DIOXABOROLAN-2-YL)-7,8-DIHYDRONAPHTHALENE-2-CARBONITRILE synthesis
- Product Name:5-(4,4,5,5-TETRAMETHYL-[1,3,2]DIOXABOROLAN-2-YL)-7,8-DIHYDRONAPHTHALENE-2-CARBONITRILE
- CAS Number:952675-93-3
- Molecular formula:C17H20BNO2
- Molecular Weight:281.16
90401-84-6
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Yield:-
Steps:
Multi-step reaction with 2 steps
1: 2,6-di-tert-butyl-4-methylpyridine / 16 h / 0 - 5 °C
2: potassium phenolate / bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine / toluene / 4 h / 50 °C
References:
SPEEDEL EXPERIMENTA AG WO2007/116098, 2007, A1