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5-(4,4,5,5-TETRAMETHYL-[1,3,2]DIOXABOROLAN-2-YL)-7,8-DIHYDRONAPHTHALENE-2-CARBONITRILE synthesis

2synthesis methods
90401-84-6 Synthesis
6-CYANO-1-TETRALONE

90401-84-6
75 suppliers
inquiry

5-(4,4,5,5-TETRAMETHYL-[1,3,2]DIOXABOROLAN-2-YL)-7,8-DIHYDRONAPHTHALENE-2-CARBONITRILE

952675-93-3
6 suppliers
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: 2,6-di-tert-butyl-4-methylpyridine / 16 h / 0 - 5 °C
2: potassium phenolate / bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine / toluene / 4 h / 50 °C

References:

SPEEDEL EXPERIMENTA AG WO2007/116098, 2007, A1