2-(3,4-DIMETHOXY-PHENYL)-5-{[2-(3,4-DIMETHOXYPHENYL)-ETHYL]METHYL-AMINO}-PENTANENITRILE synthesis
- Product Name:2-(3,4-DIMETHOXY-PHENYL)-5-{[2-(3,4-DIMETHOXYPHENYL)-ETHYL]METHYL-AMINO}-PENTANENITRILE
- CAS Number:95748-23-5
- Molecular formula:C24H32N2O4
- Molecular Weight:412.52
93-17-4
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Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: diisopropylamine; n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C
1.2: 0.33 h / -78 °C
1.3: 1 h / 22 °C
2.1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 80 °C
References:
Singh, Kawaljit;Kumar, Malkeet;Pavadai, Elumalai;Naran, Krupa;Warner, Digby F.;Ruminski, Peter G.;Chibale, Kelly [Bioorganic and Medicinal Chemistry Letters,2014,vol. 24,# 14,p. 2985 - 2990]