1H-Purine-2,6-dione, 7-[2-(acetyloxy)ethyl]-3,7-dihydro-1,3-dimethyl- synthesis
- Product Name:1H-Purine-2,6-dione, 7-[2-(acetyloxy)ethyl]-3,7-dihydro-1,3-dimethyl-
- CAS Number:96474-41-8
- Molecular formula:C11H14N4O4
- Molecular Weight:266.2533
Yield:96474-41-8 98%
Reaction Conditions:
for 8 h;Reflux;
Steps:
Ligands L7, L8, and L9 were all prepared the same way as follows:
General procedure: Ligands L7, L8, and L9 were all prepared the same way as follows: in a round bottom flask 1 mmol of L4, L5, and L6 was set to reflux in acetic anhydride (15 mL) for 8 h. After the prescribed reaction, the resulting yellow reaction mixture is cooled to room temperature and the solvent evaporated under vacuum to produce white to light yellow microcrystalline powders that can be recrystallized (CH2Cl2/hexane) for better quality products.
References:
Conelly-Espinosa, Patricia;Toscano, Ruben A.;Morales-Morales, David [Tetrahedron Letters,2014,vol. 55,# 42,p. 5841 - 5845]
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