Welcome to chemicalbook!
Chinese English Japanese Germany Korea
400-158-6606
Try our best to find the right business for you.
Do not miss inquiry messages Please log in to view all inquiry messages.

Welcome back!

ChemicalBook CAS DataBase List 4-CHLORO-2,5-DIMETHYL-2H-PYRAZOLE-3-CARBOXYLIC ACID

4-CHLORO-2,5-DIMETHYL-2H-PYRAZOLE-3-CARBOXYLIC ACID synthesis

4synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: N,N-dimethyl-formamide / 3 h / 60 °C
2: sulfuryl dichloride / 1,2-dichloro-ethane / 2 h / Reflux
3: sodium hydroxide / water / 4 h / 80 °C

References:

Huang, Danling;Huang, Mingzhi;Liu, Aiping;Liu, Xingping;Liu, Weidong;Chen, Xiaoyang;Xue, Hansong;Sun, Jiong;Yin, Dulin;Wang, Xiaoguang [Journal of Heterocyclic Chemistry,2017,vol. 54,# 2,p. 1121 - 1128]