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ChemicalBook CAS DataBase List (5-PHENYL-[1,3,4]OXADIAZOL-2-YLSULFANYL)-ACETIC ACID
99361-50-9

(5-PHENYL-[1,3,4]OXADIAZOL-2-YLSULFANYL)-ACETIC ACID synthesis

6synthesis methods
-

Yield:99361-50-9 72%

Reaction Conditions:

Stage #1: carbon disulfide;benzoic acid hydrazide in N,N-dimethyl-formamide at 20 - 70; for 4 h;
Stage #2: chloroacetic acidwith triethylamine in N,N-dimethyl-formamide at 20; for 0.916667 h;chemoselective reaction;

References:

Soleiman-Beigi, Mohammad;Alikarami, Mohammad;Hosseinzadeh, Tahereh [Asian Journal of Chemistry,2013,vol. 25,# 9,p. 4939 - 4942]

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