SODIUM P-CHLOROBENZOATE synthesis
- Product Name:SODIUM P-CHLOROBENZOATE
- CAS Number:3686-66-6
- Molecular formula:C7H4ClNaO2
- Molecular Weight:178.55
1126-46-1
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18027-10-6
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$66.00/1g
3686-66-6
48 suppliers
$40.00/500mg
Yield:3686-66-6 86%
Reaction Conditions:
in toluene
Steps:
8 Sodium 4-chlorobenzoate
EXAMPLE 8 Sodium 4-chlorobenzoate The procedure of Example 1 was followed using methyl 4-chlorobenzoate (4.55 g, 26.6 mmol), sodium trimethylsilanolate (2.99 g, 26.6 mmol), dry toluene (150 mL), and 4 h of heating at 80°. Sodium 4-chlorobenzoate (4.50 g, 86% yield) was isolated as a white solid: 1 H NMR (D2 O, DSS, 80 MHz) δ 7.65 ppm (ABq, Δν1-3 =29 Hz, J=8 Hz, Ar--H's, 4H).
References:
E. I. Du Pont de Nemours and Company US4723016, 1988, A
1126-46-1
228 suppliers
$8.00/25g
3686-66-6
48 suppliers
$40.00/500mg
4254-20-0
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3686-66-6
48 suppliers
$40.00/500mg
74-11-3
561 suppliers
$5.00/1g
3686-66-6
48 suppliers
$40.00/500mg
104-88-1
611 suppliers
$5.00/25g
3686-66-6
48 suppliers
$40.00/500mg