A-(P-TERT-BUTYLPHENOXY)PROPIONIC ACID synthesis
1synthesis methods
- Product Name:A-(P-TERT-BUTYLPHENOXY)PROPIONIC ACID
- CAS Number:16453-53-5
- Molecular formula:C13H18O3
- Molecular Weight:222.28
Yield:16453-53-5 95%
Reaction Conditions:
Stage #1: para-tert-butylphenolwith sodium hydride in N,N-dimethyl-formamide at 25 - 30; for 0.5 h;
Stage #2: 2-Bromopropionic acid in N,N-dimethyl-formamide at 20 - 25; for 4 h;
References:
Sarkar, Piyali;Mukhopadhyay, Chhanda [Green Chemistry,2015,vol. 17,# 6,p. 3452 - 3465] Location in patent:supporting information