Acetic acid, 2-(2,3,4-trifluorophenoxy)- synthesis

5synthesis methods

Product Name:Acetic acid, 2-(2,3,4-trifluorophenoxy)-
CAS Number:322-26-9
Molecular formula:C8H5F3O3
Molecular Weight:206.12

2268-05-5 Synthesis

2268-05-5
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Acetic acid, 2-(2,3,4-trifluorophenoxy)-

322-26-9
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Yield:-

Steps:

Multi-step reaction with 5 steps
1: sulfuric acid; aqueous nitric acid / 40 °C
2: dimethylformamide; potassium fluoride / 150 °C
3: iron; aqueous NH₄Cl
4: sulfuric acid; sodium nitrite; phosphoric acid / Erhitzen des Reaktionsgemisches mit Kupfer(II)-sulfat und wss. Schwefelsaeure auf 140grad
5: aq. NaOH solution

References:

Finger et al. [Journal of the American Chemical Society,1959,vol. 81,p. 94,95, 97]

771-69-7 Synthesis