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ChemicalBook CAS DataBase List ACETIC ACID 2-PROPIONYLPHENYL ESTER

ACETIC ACID 2-PROPIONYLPHENYL ESTER synthesis

6synthesis methods
Obtained by reaction of acetic anhydride with 2-hydroxypropiophenone
Also obtained by reaction of ethylmagnesium bromide with 2-acetoxybenzoyl chloride (84%).
-

Yield:97139-82-7 84%

Reaction Conditions:

with Bis<2-(N,N-dimethylamino)aethyl>aether in tetrahydrofuran;cooling;Grignard reaction;

References:

Wang, Xiao-Jun;Zhang, Li;Sun, Xiufeng;Xu, Yibo;Krishnamurthy, Dhileepkumar;Senanayake, Chris H. [Organic Letters,2005,vol. 7,# 25,p. 5593 - 5595]