ACROLEIN 2,4-DINITROPHENYLHYDRAZONE synthesis

5synthesis methods

Yield:-

Steps:

Multi-step reaction with 3 steps
1: potassium nitrate; sulfuric acid
2: hydrazine; acetic acid
3: formic acid / acetonitrile / 2 h / 40 °C / Darkness

References:

Szarka, Szabolcs;Prokai-Tatrai, Katalin;Prokai, Laszlo [Analytical Chemistry,2014,vol. 86,# 14,p. 7033 - 7040]

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