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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide

AKOS 93602 synthesis

6synthesis methods
606-27-9 Synthesis
METHYL 2-NITROBENZOATE

606-27-9
96 suppliers
$21.00/1g

75-05-8 Synthesis
Acetonitrile

75-05-8
966 suppliers
$10.00/10g

AKOS 93602

40017-83-2
17 suppliers
inquiry

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Yield:40017-83-2 69%

Reaction Conditions:

Stage #1: acetonitrilewith n-butyllithium in tetrahydrofuran;hexane at -78; for 1 h;Sealed tube;Inert atmosphere;
Stage #2: methyl 2-nitrobenzoate in tetrahydrofuran;hexane at -45; for 3.25 h;Sealed tube;Inert atmosphere;

References:

Lee, Seok Beom;Jang, Yoonkyung;Ahn, Jiwon;Chun, Simin;Oh, Dong-Chan;Hong, Suckchang [Organic Letters,2020,vol. 22,# 21,p. 8382 - 8386] Location in patent:supporting information

2-Propenoic acid, 2-cyano-3-hydroxy-3-(2-nitrophenyl)-, ethyl ester, (Z)- (9CI)

141342-35-0
0 suppliers
inquiry

AKOS 93602

40017-83-2
17 suppliers
inquiry

References
610-14-0 Synthesis
2-Nitrobenzoyl chloride

610-14-0
5 suppliers
$61.89/5g

AKOS 93602

40017-83-2
17 suppliers
inquiry

References
Benzenepropanoic acid, α-cyano-2-nitro-β-oxo-, ethyl ester

91974-26-4
0 suppliers
inquiry

AKOS 93602

40017-83-2
17 suppliers
inquiry

References
Ethanone, 2-chloro-1-(2-nitrophenyl)- (9CI)

113337-37-4
2 suppliers
inquiry

143-33-9 Synthesis
Sodium cyanide

143-33-9
5 suppliers
$10.00/1g

AKOS 93602

40017-83-2
17 suppliers
inquiry

References

AKOS 93602 Related Search:

1-NITRO-2-PROPYLBENZENE 2-Nitroacetophenone Benzoylacetonitrile