ChemicalBook CAS DataBase List AKOS B013937

AKOS B013937 synthesis

8synthesis methods

Product Name:AKOS B013937
CAS Number:17431-97-9
Molecular formula:C10H11NO5
Molecular Weight:225.2

600-00-0 Synthesis

600-00-0
262 suppliers
$13.00/5g

100-02-7 Synthesis

100-02-7
5 suppliers
$11.00/5G

17431-97-9
19 suppliers
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Yield:17431-97-9 62.8%

Reaction Conditions:

Stage #1: ethyl 2-bromoisobutyrate;4-nitro-phenolwith potassium carbonate in acetonitrile; for 8 h;Reflux;
Stage #2: with lithium hydroxide in tetrahydrofuran;methanol;water at 20; for 3 h;
Stage #3: with hydrogenchloride in tetrahydrofuran;methanol;water;

References:

Almanza-Pérez, Julio Cesar;Chávez-Silva, Fabiola;Colin-Lozano, Blanca;Estrada-Soto, Samuel;Hidalgo-Figueroa, Sergio;Navarrete-Vazquez, Gabriel;Torres-Gomez, Héctor [Pharmaceuticals,2022,vol. 15,# 1,art. no. 102]

100-02-7 Synthesis

100-02-7
5 suppliers
$11.00/5G

67-66-3 Synthesis