![](/CAS/GIF/762-67-4.gif)
ALLYLTRICHLOROGERMANE synthesis
- Product Name:ALLYLTRICHLOROGERMANE
- CAS Number:762-67-4
- Molecular formula:C3H5Cl3Ge
- Molecular Weight:220.07
Yield:762-67-4 92%
Reaction Conditions:
in neat (no solvent);to a two-necked flask with N2 inlet introduced GeCl4; Sn-compound added dropwise at room temp. for about 5 min; stirred at 40°C for 3 h; flask attached to the vacuum line equipped with a trap, which cooled at -50°C to condense the product; product distilled by heating the reaction mixture up to 40°C;
References:
Horn, Anne;Mollendal, Harald;Demaison, Jean;Petitprez, Denis;Moreno, Juan Ramon Aviles;Benidar, Abdessamad;Guillemin, Jean-Claude [Journal of Physical Chemistry A,2005,vol. 109,# 17,p. 3822 - 3829]
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