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ALPHA-(4-TOLYLIMINO)-P-CRESOL 96 synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: hydrogenchloride; sodium nitrite / water / 1 h / 0 - 5 °C / Inert atmosphere
1.2: 10 h / 20 °C / Inert atmosphere
2.1: iron(II) chloride / acetonitrile / 100 °C / Sealed tube; Inert atmosphere

References:

Peng, Yi;Fan, Yan-Hui;Li, Si-Yuan;Li, Bin;Xue, Jing;Deng, Qing-Hai [Organic Letters,2019,vol. 21,# 20,p. 8389 - 8394]