ALPHA-METHYL-L-TRYPTOPHAN synthesis
- Product Name:ALPHA-METHYL-L-TRYPTOPHAN
- CAS Number:16709-25-4
- Molecular formula:C12H14N2O2
- Molecular Weight:218.25
69876-37-5
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$11.00/1g
16709-25-4
85 suppliers
$779.63/25MG
Yield:-
Steps:
Multi-step reaction with 5 steps
1: CF3COOH / 96 h / Ambient temperature
2: Na2CO3 / dioxane; H2O / 0 °C
3: 1.) lithium bis(trimethylsilyl)amide / 1.) THF, -78 deg C, 1 h, 2.) THF, a) -78 deg C, 1 h, b) from -78 deg C to RT, 2 h
4: trifluoroacetic acid / 1.5 h / Ambient temperature
5: H2 / 10percent Pd/C / ethanol / 3 h / Ambient temperature
References:
Ekhato, I. Victor;Huang, Yun [Journal of labelled compounds and radiopharmaceuticals,1997,vol. 39,# 12,p. 1019 - 1038]
![1H-Indole-1-carboxylic acid, 3-[[(3S,5aR,6aS,7aS)-2,3,5,5a,6,6a,7,7a-octahydro-3,6,6,7a-tetramethyl-2-oxocyclopropa[g]-1,4-benzoxazin-3-yl]methyl]-, 1,1-dimethylethyl ester](/CAS/20210305/GIF/1266681-04-2.gif)
1266681-04-2
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16709-25-4
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116139-87-8
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16709-25-4
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114524-80-0
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$64.06/250MG
56452-52-9
53 suppliers
$165.00/25mg
16709-25-4
85 suppliers
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96551-27-8
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114524-80-0
67 suppliers
$64.06/250MG
16709-25-4
85 suppliers
$779.63/25MG
96551-27-8
0 suppliers
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