α-AMino-2-thiopheneacetonitrile synthesis
- Product Name:α-AMino-2-thiopheneacetonitrile
- CAS Number:61261-50-5
- Molecular formula:C6H6N2S
- Molecular Weight:138.19
Yield:61261-50-5 70%
Reaction Conditions:
Stage #1: thiophene-2-carbaldehydewith lithium hexamethyldisilazane in tetrahydrofuran at 25; for 4 h;
Stage #2: 2-hydroxy-2-methylpropanenitrile in tetrahydrofuran at 25; for 12 h;
References:
Chu, Guo-Hua;Gu, Minghua;Gerard, Baudouin;Dolle, Roland E. [Synthetic Communications,2004,vol. 34,# 24,p. 4583 - 4590]
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