(Aminomethyl)cyclohexane synthesis
- Product Name:(Aminomethyl)cyclohexane
- CAS Number:3218-02-8
- Molecular formula:C7H15N
- Molecular Weight:113.2
766-05-2
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3218-02-8
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$21.00/1mL
Yield:3218-02-8 91%
Reaction Conditions:
with hydrogen in ethanol at 88; under 37503.8 Torr; for 0.5 h;
Steps:
1 Amines Preparation Examples
In the 1L hydrogenation kettle, add 100 g of cyclohexanecarbonitrile and 3 g of Raney-Ni, 400 mL of ethanol, and continuously charged with H2, so that the pressure of the system during the reaction was always maintained at 5 MPa. After reaction at a reaction temperature of 88 ° C for 0.5 h, then the temperature was lowered. When the temperature in the reaction vessel was lowered to room temperature, the gas was vented, and c cyclohexanemethylamine (purity: 99% or more) was obtained by filtration and recrystallization in a yield of 91 wt%.
References:
Sinopec Corporation;Sinopec Yangzi Petrochemical Co., Ltd.;Sun Hailong;Wei Yanyu;Gao Yilong;Chen Xinhua;Miao Jun;Li Na;Kan Lin;Bai Jiye;Chen Shaohui;Yang Aiwu;Xu Yuexing CN104557356, 2017, B Location in patent:Paragraph 0231; 0232
2043-61-0
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3218-02-8
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$21.00/1mL
100-46-9
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$5.00/5 g
3218-02-8
148 suppliers
$21.00/1mL
86328-85-0
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3218-02-8
148 suppliers
$21.00/1mL
