ChemicalBook CAS DataBase List anhalinine

anhalinine synthesis

10synthesis methods

Product Name:anhalinine
CAS Number:642-30-8
Molecular formula:C12H17NO3
Molecular Weight:223.27

Benzenemethanamine, 2,3,4-trimethoxy-N-[2-(phenylthio)ethyl]-

221128-78-5
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642-30-8
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Yield:-

Steps:

Multi-step reaction with 5 steps
1: 98 percent / Ac₂O / 1 h / 70 °C
2: 97 percent / NaIO₄ / H₂O; methanol / 16 h / Ambient temperature
3: 99 percent / TFAA, BF₃*OEt₂ / benzene / 1 h / Ambient temperature
4: 76 percent / NaBH₄, NiCl₂*6H₂O / methanol; tetrahydrofuran / 0.5 h / Ambient temperature
5: 86 percent / 10 percent NaOH / H₂O; ethanol / 1.5 h / Heating

References:

Shinohara, Tatsumi;Takeda, Akira;Toda, Jun;Kohno, Michiyo;Sano, Takehiro [Heterocycles,1999,vol. 51,# 1,p. 119 - 129]

2(1H)-Isoquinolinecarboxaldehyde, 3,4-dihydro-6,7,8-trimethoxy-

221128-88-7
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642-30-8
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References

Formamide, N-[2-(phenylthio)ethyl]-N-[(2,3,4-trimethoxyphenyl)methyl]-

221128-80-9
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642-30-8
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References

2(1H)-Isoquinolinecarboxaldehyde, 3,4-dihydro-6,7,8-trimethoxy-4-(phenylthio)-

221128-86-5
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642-30-8
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References

Formamide, N-[2-(phenylsulfinyl)ethyl]-N-[(2,3,4-trimethoxyphenyl)methyl]-

221128-82-1
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642-30-8
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References