ara-CDP-1-S-hexadecyl-2-O-palmitoyl-1-thioglycerol synthesis

3synthesis methods

Product Name:ara-CDP-1-S-hexadecyl-2-O-palmitoyl-1-thioglycerol
CAS Number:125592-29-2
Molecular formula:C44H84N3NaO13P2S
Molecular Weight:980.16

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ara-CDP-1-S-hexadecyl-2-O-palmitoyl-1-thioglycerol

125592-29-2
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Yield:-

Steps:

Multi-step reaction with 5 steps
1: pyridine / 24 h / Heating
2: 82.4 percent / pyridine / benzene / 70 - 80 °C
3: BF₃-MeOH / CH₂Cl₂ / 1 h / 0 °C
4: 56 percent / POCl₃, triethylamine / hexane; toluene / Ambient temperature
5: 25 percent / pyridine / 240 h / Ambient temperature

References:

Il Hong;Kirisits;Nechaev;Buchheit;West [Journal of Medicinal Chemistry,1990,vol. 33,# 5,p. 1380 - 1386]

112-82-3 Synthesis

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125592-29-2
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References

2-Propanol, 1-(hexadecylthio)-3-(triphenylmethoxy)-

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125592-29-2
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References