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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide

AS1940477 Hydrobromide synthesis

9synthesis methods
AS1940477

928344-12-1
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AS1940477 Hydrobromide

1404189-10-1
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Yield:1404189-10-1 16.7 kg

Reaction Conditions:

with hydrogen bromide in propan-1-ol;water at 25 - 65; for 25 h;Large scale;

References:

Yoshida, Shinya;Hayashi, Yasumasa;Obitsu, Kazuyoshi;Nakamura, Atsushi;Kikuchi, Takashi;Sawada, Tatsuya;Kimura, Takenori;Takahashi, Takumi;Mukuta, Takashi [Organic Process Research and Development,2012,vol. 16,# 11,p. 1818 - 1826]