Benzenamine, 3-(4-pyridinyloxy)- synthesis
- Product Name:Benzenamine, 3-(4-pyridinyloxy)-
- CAS Number:102877-77-0
- Molecular formula:C11H10N2O
- Molecular Weight:186.21
4783-89-5
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Yield:102877-77-0 96%
Reaction Conditions:
with palladium on activated charcoal;hydrogen in methanol at 20; for 2 h;
Steps:
15.b Step b:
A solution of Compound 15-1 (1.8 g, 8.33 mmol) and Pd/C (200 mg) in MeOH (50 mL) was stirred at room temperature for 2hours. The reaction was filtered and concentrated under reduced pressure to give Compound 15-2 (1.5 g, 96%).
References:
WO2021/226517,2021,A1 Location in patent:Paragraph 0394; 0395
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