Benzenamine, 4-(2-propen-1-yl)- synthesis

8synthesis methods

Product Name:Benzenamine, 4-(2-propen-1-yl)-
CAS Number:32704-23-7
Molecular formula:C9H11N
Molecular Weight:133.19

53483-17-3
2 suppliers
inquiry

7439-89-6
422 suppliers
$10.00/25g

32704-23-7
2 suppliers
inquiry

Yield:-

Reaction Conditions:

with ammonium chloride in ethanol;water;

Steps:

86.B 4-allyl-phenylamine

Example 86B 4-allyl-phenylamine A solution of 1-allyl-4-nitro-benzene (1.92 g, 11.8 mmol), NH₄Cl (1.89 g, 35.3 mmol) and iron powder (4.60 g, 82.4 mmol) in 3:1 ethanol:H₂O (200 mL) was heated to reflux overnight. The reaction was cooled, concentrated under reduced pressure and purified on silica gel eluding with ethyl acetate to provide the titled compound. MS (ESI(+)) m/e 134 (M+H)⁺

References:

US2002/35137,2002,A1

24850-33-7 Synthesis