Benzene, 1,1'-methylenebis[4-(methoxymethyl)- synthesis

2synthesis methods

Product Name:Benzene, 1,1'-methylenebis[4-(methoxymethyl)-
CAS Number:32449-08-4
Molecular formula:C17H20O2
Molecular Weight:256.34

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Benzene, 1,1'-methylenebis[4-(methoxymethyl)-

32449-08-4
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Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: BuLi / tetrahydrofuran; hexane / 0.25 h / -78 °C
1.2: 76 percent / tetrahydrofuran; hexane / 0.42 h / -78 °C
2.1: 87 percent / KOH; hydrazine monohydrate / bis-(2-hydroxy-ethyl) ether / 0.33 h / 130 °C / microwave irradiation

References:

Stuhr-Hansen, Nicolai;S?rensen, Jakob Kryger;Moth-Poulsen, Kasper;Christensen, J?rn Bolstad;Bj?rnholm, Thomas;Nielsen, Mogens Br?ndsted [Tetrahedron,2005,vol. 61,# 52,p. 12288 - 12295]

Methanone, bis[4-(methoxymethyl)phenyl]-

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32449-08-4
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References