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Benzene, 1-bromo-2,5-dihexyl-4-iodo- synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 98 percent / n-BuLi / diethyl ether; hexane / 1.) -78 to 0 deg C, 2.) -78 deg C to r.t., 12 h
2: 97 percent / ICl / CCl4 / 0.5 h

References:

Hensel, Volker;Schlueter, A.-Dieter [Liebigs Annalen,1997,# 2,p. 303 - 309]