Benzene, 1-fluoro-2-(2-methyl-2-propenyl)- (9CI) synthesis
- Product Name:Benzene, 1-fluoro-2-(2-methyl-2-propenyl)- (9CI)
- CAS Number:731772-97-7
- Molecular formula:C10H11F
- Molecular Weight:150.19
462-06-6
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$10.00/5g
563-47-3
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731772-97-7
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$252.00/1g
Yield:731772-97-7 43%
Reaction Conditions:
with di-tert-butyl(2-methoxyphenyl)phosphine;palladium diacetate;silver pivalate;caesium carbonate in neat (no solvent) at 120; for 17 h;Inert atmosphere;Sealed tube;regioselective reaction;
References:
Lee, Sarah Yunmi;Hartwig, John F. [Journal of the American Chemical Society,2016,vol. 138,# 46,p. 15278 - 15284] Location in patent:supporting information