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Benzene, (2-bromobutyl)- synthesis

3synthesis methods
-

Yield:81012-82-0 75%

Reaction Conditions:

with 1H-imidazole;bromine;triphenylphosphine in dichloromethane at 20; for 17 h;Inert atmosphere;Sealed tube;Cooling with ice;

References:

Dupuy, Stéphanie;Zhang, Ke-Feng;Goutierre, Anne-Sophie;Baudoin, Olivier [Angewandte Chemie - International Edition,2016,vol. 55,# 47,p. 14793 - 14797][Angew. Chem.,2016,vol. 128,# 47,p. 15013 - 15017,5] Location in patent:supporting information