ChemicalBook CAS DataBase List Benzene, 2-iodo-4-Methoxy-1-Methyl-

Benzene, 2-iodo-4-Methoxy-1-Methyl- synthesis

4synthesis methods

Product Name:Benzene, 2-iodo-4-Methoxy-1-Methyl-
CAS Number:260558-14-3
Molecular formula:C8H9IO
Molecular Weight:248.06

50868-72-9 Synthesis

50868-72-9
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260558-14-3
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Yield:260558-14-3 75%

Reaction Conditions:

Stage #1: 5-methoxy-o-toluidinewith sulfuric acid in water at 0;
Stage #2: with sodium nitrite in water at 0 - 5;
Stage #3: with potassium iodide in water at 20 - 100; for 2 h;Further stages.;

References:

Teply, Filip;Stara, Irena G.;Stary, Ivo;Kollarovic, Adrian;Lustinec, Daniel;Krausova, Zuzana;Saman, David;Fiedler, Pavel [European Journal of Organic Chemistry,2007,# 25,p. 4244 - 4250]

104-93-8 Synthesis