![](/CAS/GIF/175532-13-5.gif)
BENZENEETHANIMIDAMIDE, 3-CHLORO-N-HYDROXY- synthesis
- Product Name:BENZENEETHANIMIDAMIDE, 3-CHLORO-N-HYDROXY-
- CAS Number:175532-13-5
- Molecular formula:C8H9ClN2O
- Molecular Weight:184.62
![3-Chlorobenzyl cyanide](/CAS/GIF/1529-41-5.gif)
1529-41-5
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175532-13-5
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Yield:175532-13-5 100%
Reaction Conditions:
with hydroxylamine hydrochloride;sodium in methanol;
Steps:
52.I I.
I. 7-(3-(3-Chlorophenylmethyl)-1,2,4-oxadiaz-5-y))-1-(4-methylpiperazin-1-yl)naphthalene Sodium (0.120 g, 5.2 mol), hydroxylamine hydrochloride (0.35 g, 5.0 mmol), and (3-chlorophenyl)acetonitrile (0.303 g, 2.0 mmol) and methanol (5 mL) were used to prepare (3-chlorophenyl)acetamidoxime (0.42 g, >100%) as described above.
References:
US6166020,2000,A