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Benzenesulfonamide, 2-(methylamino)- (9CI) synthesis

4synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 85 percent / CHCl3 / 0 - 22 °C
2: 78 percent / methanol / 24 h / Heating
3: 21 percent / NaBH4 / propan-2-ol / 3 h / Ambient temperature

References:

Schlaepfer-Daehler, Marlise;Heimgartner, Heinz [Helvetica Chimica Acta,1993,vol. 76,# 6,p. 2398 - 2406]

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