Benzenesulfonamide, 4-hydroxy-N-(4-methylphenyl)- synthesis

5synthesis methods

Product Name:Benzenesulfonamide, 4-hydroxy-N-(4-methylphenyl)-
CAS Number:76410-74-7
Molecular formula:C13H13NO3S
Molecular Weight:263.31

1576-43-8
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1-Butanesulfonic acid, 1,1,2,2,3,3,4,4,4-nonafluoro-, 4-methylphenyl ester

93131-73-8
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Benzenesulfonamide, 4-hydroxy-N-(4-methylphenyl)-

76410-74-7
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Yield:76410-74-7 83%

Reaction Conditions:

with potassium phosphate;tris-(dibenzylideneacetone)dipalladium⁽⁰⁾;tert-butyl XPhos in tert-Amyl alcohol at 90; for 15 h;Inert atmosphere;

References:

Shekhar, Shashank;Dunn, Travis B.;Kotecki, Brian J.;Montavon, Donna K.;Cullen, Steven C. [Journal of Organic Chemistry,2011,vol. 76,# 11,p. 4552 - 4563] Location in patent:experimental part

4-Methoxy-N-(4-Methylphenyl)benzenesulfonaMide, 97%

7230-54-8
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76410-74-7
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References

106-44-5 Synthesis

106-44-5
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76410-74-7
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References

98-68-0
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References

106-49-0
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$5.00/5G

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References