BenzenesulfonaMide, N-(3,5-dibroMo-2-pyridinyl)- synthesis
- Product Name:BenzenesulfonaMide, N-(3,5-dibroMo-2-pyridinyl)-
- CAS Number:1111637-62-7
- Molecular formula:C11H8Br2N2O2S
- Molecular Weight:392.07
35486-42-1
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Yield: 72%
Reaction Conditions:
Stage #1:2-amino-3,5-dibromopyridine with sodium hydride in tetrahydrofuran;mineral oil at 0 - 25; for 1 h;Inert atmosphere;
Stage #2:benzenesulfonyl chloride in tetrahydrofuran;mineral oil at 25; for 24 h;Inert atmosphere;
References:
Nickel, Johannes;Fernández, Maitane;Klier, Lydia;Knochel, Paul [Chemistry - A European Journal,2016,vol. 22,# 40,p. 14397 - 14400] Location in patent:supporting information