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62646-09-7

BENZO[1,3]DIOXOL-5-YL-HYDRAZINE synthesis

2synthesis methods
14268-66-7 Synthesis
3,4-(Methylenedioxy)aniline

14268-66-7
262 suppliers
$20.00/5G

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Yield:62646-09-7 26%

Reaction Conditions:

Stage #1: benzo[1,3]dioxolo-5-ylaminewith hydrogenchloride;sodium nitrite in water at 0; for 0.5 h;
Stage #2: with hydrogenchloride;tin(ll) chloride in water at 15; for 0.5 h;

References:

Kim, Dae-Kee;Kim, Joonseop;Park, Hyun-Ju [Bioorganic and Medicinal Chemistry,2004,vol. 12,# 9,p. 2013 - 2020]

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