ChemicalBook CAS DataBase List BENZO[B]THIOPHEN-2-YLMETHYL-AMMONIUM CHLORIDE

BENZO[B]THIOPHEN-2-YLMETHYL-AMMONIUM CHLORIDE synthesis

3synthesis methods

Product Name:BENZO[B]THIOPHEN-2-YLMETHYL-AMMONIUM CHLORIDE
CAS Number:247570-04-3
Molecular formula:C9H10ClNS
Molecular Weight:199.7

6314-42-7 Synthesis

6314-42-7
51 suppliers
$46.00/1g

BENZO[B]THIOPHEN-2-YLMETHYL-AMMONIUM CHLORIDE

247570-04-3
31 suppliers
$45.00/5mg

Yield:247570-04-3 88%

Reaction Conditions:

Stage #1: benzo[b]thiophene-2-carboxamidewith triethyl borane;phenylsilane;potassium acetate in tetrahydrofuran;tert-butyl methyl ether at 120;Inert atmosphere;Schlenk technique;Sealed tube;
Stage #2: with hydrogenchloride in ethyl acetate at 20; for 8 h;Inert atmosphere;chemoselective reaction;

References:

Yao, Wubing;Fang, Huaquan;He, Qiaoxing;Peng, Dongjie;Liu, Guixia;Huang, Zheng [Journal of Organic Chemistry,2019]

3541-37-5 Synthesis

3541-37-5
183 suppliers
$14.00/1g

247570-04-3
31 suppliers
$45.00/5mg

References

55219-11-9
74 suppliers
$21.00/100mg

247570-04-3
31 suppliers
$45.00/5mg

108439-67-4
24 suppliers
$45.00/50mg

References

BENZO[B]THIOPHEN-2-YLMETHYL-AMMONIUM CHLORIDE Related Search:

3-CHLOROBENZO[B]THIOPHENE-2-CARBOXAMIDE