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ChemicalBook CAS DataBase List benzo[b]thiophen-3-yl acetate

benzo[b]thiophen-3-yl acetate synthesis

12synthesis methods
-

Yield:24434-82-0 89%

Reaction Conditions:

Stage #1: N,N-diethyl-2-methylsulfanylbenzamidewith lithium diisopropyl amide in tetrahydrofuran at -78 - 20;
Stage #2: acetyl chloridewith sodium hydride in tetrahydrofuran at 20;

References:

Pradhan, Tarun Kanti;De, Asish [Tetrahedron Letters,2005,vol. 46,# 9,p. 1493 - 1495]