Benzo[b]thiophen-5-amine, 3-methyl- synthesis

2synthesis methods

Product Name:Benzo[b]thiophen-5-amine, 3-methyl-
CAS Number:19404-20-7
Molecular formula:C9H9NS
Molecular Weight:163.24

19404-18-3
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$24.00/1g

19404-20-7
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Yield:19404-20-7 90%

Reaction Conditions:

with ammonium hydroxide;potassium phosphate;copper(l) iodide;N¹,N²-bis(5-methyl-[1,1'-biphenyl]-2-yl)oxalamide in water;dimethyl sulfoxide at 110; for 24 h;Inert atmosphere;

References:

Fan, Mengyang;Zhou, Wei;Jiang, Yongwen;Ma, Dawei [Organic Letters,2015,vol. 17,# 23,p. 5934 - 5937] Location in patent:supporting information

17514-62-4
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19404-20-7
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References