ChemicalBook CAS DataBase List BENZO(C)ACRIDINE

BENZO(C)ACRIDINE synthesis

8synthesis methods

Product Name:BENZO(C)ACRIDINE
CAS Number:225-51-4
Molecular formula:C17H11N
Molecular Weight:229.28

66-99-9 Synthesis

66-99-9
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225-51-4
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$597.00/100mg

Yield:-

Steps:

Multi-step reaction with 4 steps
1.1: isopropylmagnesium chloride / tetrahydrofuran / 0.5 h / -40 - -20 °C / Inert atmosphere
1.2: -20 - 20 °C / Inert atmosphere
2.1: iodine; acetic acid; hypophosphorous acid / water / 60 °C
3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / 0 - 20 °C
4.1: triphenylphosphine; sodium azide / N,N-dimethyl acetamide; water / 0.5 h / 120 °C / Inert atmosphere; Schlenk technique
4.2: 48 h / 120 °C / Inert atmosphere; Schlenk technique

References:

Wang, Ming;Fan, Qiaoling;Jiang, Xuefeng [Organic Letters,2018,vol. 20,# 1,p. 216 - 219]