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67648-15-1

Benzoic acid, 3-chloro-2-ethyl- synthesis

1synthesis methods
-

Yield:67648-15-1 41%

Reaction Conditions:

with N,N,N,N,-tetramethylethylenediamine;sec.-butyllithium in tetrahydrofuran;1.) -90 deg C, 30 min, 2.) -78 deg C;

References:

Bennetau, Bernard;Mortier, Jacques;Moyroud, Joel;Guesnet, Jean-Luc [Journal of the Chemical Society. Perkin transactions I,1995,# 10,p. 1265 - 1272]