![](/CAS/20200401/GIF/1345866-66-1.gif)
Benzoic acid, 4-(6-methyl-1,2,4,5-tetrazin-3-yl)- synthesis
- Product Name:Benzoic acid, 4-(6-methyl-1,2,4,5-tetrazin-3-yl)-
- CAS Number:1345866-66-1
- Molecular formula:C10H8N4O2
- Molecular Weight:216.2
Yield:1345866-66-1 82%
Reaction Conditions:
Stage #1: 4-cyanobenzoic Acid;acetonitrilewith zinc trifluoromethanesulfonate;hydrazine hydrate at 60; for 13 h;Inert atmosphere;
Stage #2: with hydrogenchloride;sodium nitrite in water at 20; pH=3;
References:
Linden, Greta;Zhang, Lei;Pieck, Fabian;Linne, Uwe;Kosenkov, Dmitri;Tonner, Ralf;Vázquez, Olalla [Angewandte Chemie - International Edition,2019,vol. 58,# 37,p. 12868 - 12873][Angew. Chem.,2019,vol. 131,p. 13000 - 13005,6] Location in patent:supporting information
![4-Cyanobenzoic acid](/CAS/GIF/619-65-8.gif)
619-65-8
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![Benzoic acid, 4-(6-methyl-1,2,4,5-tetrazin-3-yl)-](/CAS/20200401/GIF/1345866-66-1.gif)
1345866-66-1
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