ChemicalBook CAS DataBase List Benzoic acid, 4-(6-methyl-1,2,4,5-tetrazin-3-yl)-

Benzoic acid, 4-(6-methyl-1,2,4,5-tetrazin-3-yl)- synthesis

2synthesis methods

Product Name:Benzoic acid, 4-(6-methyl-1,2,4,5-tetrazin-3-yl)-
CAS Number:1345866-66-1
Molecular formula:C10H8N4O2
Molecular Weight:216.2

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75-05-8 Synthesis

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Benzoic acid, 4-(6-methyl-1,2,4,5-tetrazin-3-yl)-

1345866-66-1
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Yield:1345866-66-1 82%

Reaction Conditions:

Stage #1: 4-cyanobenzoic Acid;acetonitrilewith zinc trifluoromethanesulfonate;hydrazine hydrate at 60; for 13 h;Inert atmosphere;
Stage #2: with hydrogenchloride;sodium nitrite in water at 20; pH=3;

References:

Linden, Greta;Zhang, Lei;Pieck, Fabian;Linne, Uwe;Kosenkov, Dmitri;Tonner, Ralf;Vázquez, Olalla [Angewandte Chemie - International Edition,2019,vol. 58,# 37,p. 12868 - 12873][Angew. Chem.,2019,vol. 131,p. 13000 - 13005,6] Location in patent:supporting information

619-65-8
351 suppliers
$9.00/1g

1345866-66-1
21 suppliers
inquiry

References