Benzoyl chloride, 3-(1-methylethyl)- (9CI) synthesis
- Product Name:Benzoyl chloride, 3-(1-methylethyl)- (9CI)
- CAS Number:325770-58-9
- Molecular formula:C10H11ClO
- Molecular Weight:182.6467
5651-47-8
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Yield:325770-58-9 91%
Reaction Conditions:
with thionyl chloride at 100; for 2 h;
Steps:
108 1-(1-aza-bicyclo[2.2.2]oct-3-yl)-3-[1-(3-isopropyl-phenyl)-cyclopropyl]-urea
A mixture of 3-isopropyl-benzoic acid (5.00 g, 30.4 mmol) in SOCl2 (50 ml) was stirred at 100° C. for 2 h.
The reaction mixture was concentrated to give 3-isopropyl-benzoyl chloride (5.00 g, 91%).
References:
US9126993,2015,B2 Location in patent:Page/Page column 105
5433-01-2
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30951-66-7
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