Benzyl 2-Ethoxy-2-methylpropanoate synthesis
- Product Name:Benzyl 2-Ethoxy-2-methylpropanoate
- CAS Number:1000296-72-9
- Molecular formula:C13H18O3
- Molecular Weight:222.28
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Yield:1000296-72-9 47%
Reaction Conditions:
with sodium hydride in N,N-dimethyl-formamide at 0;
Steps:
2.2
In steps 1-4, 2-hydroxy-isobutyric acid was protected with benzyl bromide, alkylated with ethyl iodide, deprotected, and esterified to afford 2-ethoxy-isobutyric acid chloromethyl ester.
References:
US2008/9474,2008,A1 Location in patent:Page/Page column 19
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