ChemicalBook CAS DataBase List Benzyl 4-C-Nitromethylene--D-arabinopyranoside

Benzyl 4-C-Nitromethylene--D-arabinopyranoside synthesis

1synthesis methods

Product Name:Benzyl 4-C-Nitromethylene--D-arabinopyranoside
CAS Number:383173-64-6
Molecular formula:C13H17NO7
Molecular Weight:299.2766

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Benzyl 4-C-Nitromethylene--D-arabinopyranoside

383173-64-6
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Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: (Bu₃Sn)2O; molecular sieves 3 Angstroem / CHCl₃ / 3.5 h / Heating
1.2: 91 percent / Br₂ / CHCl₃ / 0.05 h / 0 °C
2.1: 43 percent / Et₃N / 1 h / 0 °C

References:

Andersch, Jens;Bols, Mikael [Chemistry - A European Journal,2001,vol. 7,# 17,p. 3744 - 3747]