![](/CAS/GIF/13035-61-5.gif)
beta-D-Ribofuranose 1,2,3,5-tetraacetate synthesis
- Product Name:beta-D-Ribofuranose 1,2,3,5-tetraacetate
- CAS Number:13035-61-5
- Molecular formula:C13H18O9
- Molecular Weight:318.28
![Acetanilide](/CAS/GIF/103-84-4.gif)
103-84-4
344 suppliers
$12.00/100g
![Inosine](/CAS/GIF/58-63-9.gif)
58-63-9
627 suppliers
$5.00/25g
![beta-D-Ribofuranose 1,2,3,5-tetraacetate](/CAS/GIF/13035-61-5.gif)
13035-61-5
555 suppliers
$5.00/25g
Yield:13035-61-5 95%
Reaction Conditions:
with aluminum (III) chloride in methanol at 60; for 2 h;Solvent;Temperature;
Steps:
1
Into a 1000 ml reaction flask, 100 g of inosine and 500 ml of methanol were added, and 202 g of acetanilide and 10 g of aluminum trichloride were added under stirring. The reaction was heated to 60° C. for 2 hours, and the organic solvent was distilled off under reduced pressure to obtain tetraacetyl ribose 112.8 g. The rate was 95% and the HPLC purity was 99.76%.
References:
CN107722090,2018,A Location in patent:Paragraph 0022; 0026; 0038
![α-D-Ribofuranose, 1,2-O-(1-methylethylidene)-, 3,5-diacetate](/CAS/20211123/GIF/37077-82-0.gif)
37077-82-0
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![Acetic anhydride](/CAS/20180808/GIF/108-24-7.gif)
108-24-7
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$14.00/250ML
![beta-D-Ribofuranose 1,2,3,5-tetraacetate](/CAS/GIF/13035-61-5.gif)
13035-61-5
555 suppliers
$5.00/25g
![Ribavirin Impurity M](/CAS/20211123/GIF/50730-26-2.gif)
50730-26-2
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![beta-D-Ribofuranose (9CI)](/CAS/GIF/36468-53-8.gif)
36468-53-8
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![Acetic anhydride](/CAS/20180808/GIF/108-24-7.gif)
108-24-7
5 suppliers
$14.00/250ML
![beta-D-Ribofuranose 1,2,3,5-tetraacetate](/CAS/GIF/13035-61-5.gif)
13035-61-5
555 suppliers
$5.00/25g
![Ribavirin Impurity M](/CAS/20211123/GIF/50730-26-2.gif)
50730-26-2
19 suppliers
inquiry