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ChemicalBook CAS DataBase List Bis-(3-chloro-propyl)-amine
102073-95-0

Bis-(3-chloro-propyl)-amine synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 92 percent / H2 / 10percent Pd/C / methanol / 2 h / 2280 Torr
2: 80 percent / SOCl2 / CH2Cl2 / 1.) room temp., overnight, 2.) reflux, 2 h

References:

Groth, Andrew M.;Lindoy, Leonard F.;Meehan, George V. [Journal of the Chemical Society. Perkin transactions I,1996,# 13,p. 1553 - 1558]